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In this tutorial, the instructor explains how to split data resulting from analysis, such as Cyril D BT S RF Raman spectroscopy and FTIR, into Y and X axes. The process involves opening the data in Notepad, copying it, pasting it into Microsoft Excel, and recognizing that the data cannot be plotted directly in X and Y columns. The data needs to be split into separate X and Y components for proper visualization and analysis.