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MSHA - Standard Test Procedure - Determination of Water in Hydraulic Fluid Using the Karl Fischer Ti

MSHA - Standard Test Procedure - Determination of Water in Hydraulic Fluid Using the Karl Fischer Ti 2025

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The document ASTP 5001 outlines the Standard Test Method for determining water content in hydraulic fluid using the Karl Fischer Titration Method, as established by the Mine Safety and Health Administration (MSHA). It details the purpose, scope, definitions, required equipment, procedures for testing, and criteria for pass/fail results. The method is applicable to MSHA approved Fire-Resistant Hydraulic Fluids and includes specific instructions for sample preparation, titration processes, and data recording.

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What is the Karl Fischer method of water content test?

Karl Fischer Titration is a technique for the determination of moisture content. The technique was developed by a chemist named Karl Fischer. It is based on a reagent which reacts with water and converts the water into a non-conductive chemical.

What is Karl Fischers method used for?

Karl Fischer titration is a titration method that uses volumetric or coulometric titration to determine the quantity of water present in a given analyte.

What is the KF test for water?

In analytical chemistry, Karl Fischer titration is a classic titration method that uses coulometric or volumetric titration to determine trace amounts of water in a sample. It was invented in 1935 by the German chemist Karl Fischer. Today, the titration is done with an automated Karl Fischer titrator.

What is the general method of determination of water Karl Fischer method?

Take a suitable quantity of sample specimen having 5-30 mg of water, transfer the sample quickly into the titration vessel, dissolve it in the solution by stirring, add an excessive and definite volume of Karl Fischer TS, and then titrate the solution with the standard water-methanol solution to the end point under

What is the Karl Fischer method of determining water content determination?

Water determination with Karl Fischer titration In the volumetric method a Karl Fischer solution containing iodine is added until the first trace of excess iodine is present. The amount of iodine converted is determined from the burette volume of the iodine-containing Karl Fischer solution.

What is the KF method for moisture content?

The Karl Fischer Titration test directly measures the water in a sample and nothing else. In the KF Method, the percentage of moisture is determined by automated potentiometric titration with an iodine and sulfur dioxide reagent. Liquid is extracted into an appropriate solvent and is titrated volumetrically.

How does KF titration work?

In volumetric KF titration, a known volume of titrant solution is added to the sample until the water content is completely reacted. The amount of titrant used is then determined, and the water content is calculated from the reaction stoichiometry.

MSHA - Standard Test Procedure - Determination of Water in Hydraulic Fluid Using the Karl Fischer Ti 2025

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