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How to work in shape in XPS

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Charles Zona (CZ): Hello, and welcome to another McCrone Group webinar. My name is Charles Zona, and today we are happy to welcome Doug Meier. Doug is going to talk to us about X-ray photoelectron spectroscopy, otherwise known as XPS. Before we get started I would like to give you a bit of Dougamp;#39;s background. Doug is a senior research scientist with McCrone Associates. He specializes in surface sensitive spectroscopies, such as Auger electron, X-ray photoelectron, infrared reflection absorption, thermal desorption, and low-energy electron diffraction. Doug was awarded the U.S. Department of Commerceamp;#39;s Silver Medal for his work in the development of conductometric chemical microsensor array technology for the detection of chemical warfare agents. He also has over ten years of micro beam analysis experience prior to joining McCrone Associates. Doug will field questions from the audience immediately following todayamp;#39;s presentation, and this webinar is being recorded

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What are the limitations of XPS?

Because XPS is a surface technique, there is a limited amount of organic information XPS can provide. XPS is limited to measurements of elements having atomic numbers of 3 or greater, making it unable to detect hydrogen or helium. XPS spectra also take a long time to obtain.

What are the disadvantages of XPS foam?

Cons of XPS: Higher cost compared to EPS. Heavier weight, which can make it more difficult to handle and . Lower R-value per inch of thickness compared to EPS.

How far does XPS penetrate?

X-Ray Photoelectron Spectroscopy is used to determine quantitative atomic composition and chemistry. It is a surface analysis technique with a sampling volume that extends from the surface to a depth of approximately 50-100 .

What is the working principle of XPS?

It is a quantitative spectroscopic technique which utilises core level shift to obtain information on the chemical and electronic state of a samples elemental components to a penetration depth of ~ 10-100 . When a photon of energy (h) penetrates the surface of a solid it is absorbed by an electron.

What are the limitations of photoelectron spectrometry?

Additionally, photoelectron spectroscopy is limited to information about the surfaces of materials, because it is dependent on the dislodged photoelectron traveling from the material to the detector, which grows less likely the more material the electron must travel through.

Which elements Cannot be detected by XPS?

Both hydrogen and helium cannot be detected using XPS. For this reason, XPS can provide only relative, rather than absolute, ratios of elements in a sample.

What does a shift in XPS peak mean?

The main cause of the peak shift in XPS spectra is mostly related to chemical shifts due to the presence or absence of the chemical states of the element having different formal oxidation state. And the intensity may also be changed bcos it is directly linked to the number of atoms in the respective chemical state.

What is the work function of the spectrometer in XPS?

The work function is a correction factor for the instrument and correlates to the minimum energy required to eject an electron from an atom (see the photoelectric effect for more info, but not necessary to understand this).

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