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in this video weamp;#39;re going to explore the consequences for xps spectra that are measured from samples that have been prepared in different ways with the identical material the sample that weamp;#39;re measuring by xps is an aluminium foil that has an oxide layer then a metallic aluminium and the underside is also an oxide layer and the difference between how these samples are being prepared is whether or not this sample is electrically connected to the sample holder and whether the bottom or the top of the sample is electrically connected or in the third case where the sample is isolated from the sample holder and this is the situation where charge compensation will be required to maintain a steady potential for this sample the first observation one would make looking at these three different spectra measured from three different samples is that all three have a similar shape that is to say an aluminium oxide peak that is relatively broad and then a relatively narrow metallic p
