Tack period in XPS

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How to tack period in XPS

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Charles Zona (CZ): Hello, and welcome to another McCrone Group webinar. My name is Charles Zona, and today we are happy to welcome Doug Meier. Doug is going to talk to us about X-ray photoelectron spectroscopy, otherwise known as XPS. Before we get started I would like to give you a bit of Dougamp;#39;s background. Doug is a senior research scientist with McCrone Associates. He specializes in surface sensitive spectroscopies, such as Auger electron, X-ray photoelectron, infrared reflection absorption, thermal desorption, and low-energy electron diffraction. Doug was awarded the U.S. Department of Commerceamp;#39;s Silver Medal for his work in the development of conductometric chemical microsensor array technology for the detection of chemical warfare agents. He also has over ten years of micro beam analysis experience prior to joining McCrone Associates. Doug will field questions from the audience immediately following todayamp;#39;s presentation, and this webinar is being recorded

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What does a shift in XPS mean?

In general, it is known that for most materials, when the XPS peak becomes higher shift, it means strong bonding with oxidation, and conversely, when the electron concentration increases, it is known that it is referred to as lower shift.

What is the Beer Lambert law of XPS?

The intensity of photoelectrons emitted at the surface (Is) is determined by the Beer-Lambert Law: Is = Ioe-d/ where Iois the intensity of the photoelectrons emitted at depth d below the surface and is the inelastic mean free path of the electron in the material.

What is attenuation length in XPS?

The electron attenuation length (AL) is commonly understood to be a measure of the opacity of a solid for a given electron energy in surface-sensitive spectroscopies such as Auger-electron spectroscopy (AES) and X-ray photoelectron spectroscopy (XPS).

What causes the peak shift in XPS?

The main cause of the peak shift in XPS spectra is mostly related to chemical shifts due to the presence or absence of the chemical states of the element having different formal oxidation state. And the intensity may also be changed bcos it is directly linked to the number of atoms in the respective chemical state.

What is the blue shift in nanoparticle luminescence?

Blue shift or hypsochromic effect can be attributed to absorption to shorter wavelength due to reduction in particle size and higher surface plasmon resonance energy.

What is the significance of the blue shift?

Doppler blueshift is used in astronomy to determine relative motion: The Andromeda Galaxy is moving toward our own Milky Way galaxy within the Local Group. When observed from earth, its light shows a blueshift. Components of a binary star system will be blueshifted when moving towards Earth.

What is the blue shift in XPS?

The blue curve indicates a 5-year derivative. The strength of the XPS technique relies on that the chemical environment of an atom has a pronounced effect on the assessed binding energies (BEs) of core-level electrons, the effect commonly referred to as the chemical shift [2].

What is red shift and blue shift in Raman spectra?

A blue shift is any decrease in wavelength, with a corresponding increase in frequency, of an electromagnetic wave; the opposite effect is referred to as red shift. Basically red shift means that frequency of phonons interacting with the incident photon decreased, blue shift means that it increased.

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