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energy calibration is performed window under the calibration property page and the idea of Mg calibrating and XPS spectrum is that you perform a shift and the ship should be applied to all measurements that are made at the same time that is to say youve got a set of oxygen Peaks here where you can see shifts are evident and each one of these rows represents a different measurement so if we look at the molybdenum say you can see that theres a similar sort of shift going on here and what about the carbon yes youve got again similar shift here so these shifts in the energy are consistent along these rows and the idea of the calibration is to work out what that shift needs to be to align all these Peaks now one question might be that why do you get shifts in xbs Peaks and an explanation but a charge builds up on the sample because when you array d8 the sample with x-rays electrons are being extracted and these are the basis for the spectra that were measuring and this represents a cur
