Inject side in XPS smoothly

Aug 6th, 2022
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How to Inject side in XPS

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this video is an introduction to xps xps is most often viewed through the analysis of xps data which involves using software to work out quantification and chemical state information based on spectra that are gathered from samples but to properly understand how the sample is analyzed in terms of the software its important to have some appreciation of the xps technique itself so this involves having an understanding of what were looking at in terms of energy spectra and also how spectra are acquired that will then be processed to produce the information that were after an xps spectrum is an energy spectrum and the energy spectrum is acquired by changing the energy at which we sample the number of electrons that arrive at a detector and as a consequence of these types of measurements we can create a histogram of intensity as a function of energy here its plotted as intensity as a function of binding energy and the binding energy is related to an electronic configuration with an atom

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Shake-up satellites: distinct peaks a few eV below the main line. Shake-off satellites: broad feature at lower energy w.r.t. to main line. energy loss). n: e density, e: charge of e, m: mass of e electron.
At room temperature, kT is approximately 0.025 eV. Using equation (1), this means that the instrument resolution is 0.258 eV. Using this instrumental resolution and the Ag 3d5/2 natural line width and applying equation (1) again, the experimental peak width can be calculated to be 0.42 eV.
Chemical shift arises in the initial state from the displacement of the electronic charge from the atom towards its ligands, reducing the electrostatic potential at the atom. There is a final state shift due to the polarization of the ligand by the core on the central atom.
Temperature Gradients Within Columns (The temperature is lower at the center of the column than near the column inner walls.) That can cause peak broadening.
The main cause of the peak shift in XPS spectra is mostly related to chemical shifts due to the presence or absence of the chemical states of the element having different formal oxidation state. And the intensity may also be changed bcos it is directly linked to the number of atoms in the respective chemical state.
That is, broadening of a peak may indicate: a change in the number of chemical bonds contributing to a peak shape, a change in the sample condition (x-ray damage) and/or differential charging of the surface (localised differences in the charge state of the surface).
The intensity depends on the X-ray emission, charge neutralization, resolution, sample itself and many other parameters. So it may happen that withn the same sample and using same setting you would get a different peak intensity if you measure them on different date/time.
XPS is a surface sensitive technique because only those electrons generated near the surface escape and are detected. The photoelectrons of interest have relatively low kinetic energy.

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