Inject sample in XPS

Utilize this fast guide to inject sample in XPS with swift ease

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inject sample in XPS by reading these steps:

Register your DocHub account or log in if you already have one.
Click the Add New button to upload or import your XPS into the editor. In addition, you can take advantage of the tools available to tweak the text and customize the layout.
Select the ability to inject sample in XPS from the menu bar and use it to the form.
Check your form again to make sure you haven’t overlooked any mistakes or typos. When you finish, click on DONE.
You can then share your document with others or send it out using your preferred way.

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How to inject sample in XPS

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welcome my name is Carrie Donnelly and Iamp;#39;m the director of The Chapel Hill analytical and Nano fabrication lab or Channel at UNC today Iamp;#39;m joined by Catherine McInnis a graduate student at UNC who will be showing you how to prepare samples for x-ray photoelectron spectroscopy or XPS hello Carrie the samples that weamp;#39;ll be analyzing are carbon films on Silicon substrates both the silicon and the carbon are conductive which is ideal for XPS in my research Iamp;#39;m trying to modify the top layer of carbon atoms by attaching different atoms like chlorine and sulfur to the surface and XPS is an ideal technique to determine if Iamp;#39;ve been successful my research is focused on trying to use these surfaces to produce hydrogen gas a renewable source of energy my samples are in the lab so letamp;#39;s go there now here are my XPS samples in the sample bar that I will attach them to because XPS is so surface sensitive I want to make sure that I donamp;#39;t touch

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What can XPS tell us about a sample?

X-ray photoelectron spectroscopy (XPS), also known as electron spectroscopy for chemical analysis (ESCA), is a technique for analyzing a materials surface chemistry. XPS can measure elemental composition as well as the chemical and electronic state of the atoms within a material.

What is the sample size for XPS?

The sample size requirements are instrument dependent. The maximum sample size that can be analyzed in most XPS instruments is on the order of 20 cm2 and often on the order of a few cm2. Allowed sample heights are also instrument dependent, but typically are 25 mm.

Why are tweezers used during XPS sample preparation?

XPS can detect submonolayer coverages, so proper sample handling is essential. As mentioned above, gloves should be worn and clean metal tweezers used to handle the sample without contacting the area of interest.

What are the limitations of XPS?

Because XPS is a surface technique, there is a limited amount of organic information XPS can provide. XPS is limited to measurements of elements having atomic numbers of 3 or greater, making it unable to detect hydrogen or helium. XPS spectra also take a long time to obtain.

How to prepare a sample for XPS?

XPS Sample Preparation: Press the powder into clean, high purity indium foil. Dissolve the powder in a suitable solvent and then drop cast onto the surface of a clean silicon wafer. Sprinkle the powder onto the surface of sticky carbon conductive tape or pressed into a tablet for analysis.

Is XPS non-destructive?

The XPS (X-ray Photoelectron Spectroscopy) is one of the typical non-destructive analyzing methods.

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