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hello today Iamp;#39;m going to show you how to prepare a sample to run in our nuclear magnetic resonance spectrometers the equipment youamp;#39;ll need is shown here this includes a cleaned and dried NMR tube and cap a new pesto pipette and clean bulb a clean and dry sample while and if further filtration is required a second Pasteur pipette and a small amount of paper towel Iamp;#39;m going to start by adding a small amount of sample to the sample file approximately five to ten milligrams but if more is available it can be used if the sample to be analyzed is carbon-13 a larger quantity of pure dry product is required minimum amount of 30 milligrams is required as the default experiment to give a good signal-to-noise ratio to this sample Iamp;#39;m going to add approximately one milliliter of solvent and mix it thoroughly Iamp;#39;m using deuterated chloroform as my solvent as the deuterium offsets the effect of natural drift in the magnetic field of the NMR the solvent Iamp;#3