Clear up bates in XPS

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Aug 6th, 2022
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How to clear up bates in XPS

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Laboratory based XPS The resulting wavelength is 8.3386 angstroms (0.83386 nm) corresponding to a 1486.7 eV photon energy. Aluminum K X-rays have an intrinsic full width at half maximum (FWHM) of 0.43 eV, centered at 1486.7 eV (E/E = 3457).
While the photon energy of the monochromatic Al K x-ray source most commonly used in traditional XPS instruments is 1486.6 eV, the photon energy of the excitation source used in hard x-ray photoelectron spectroscopy is 5 to 8 keV, more than triple.
XPS is more commonly used than UPS and is often be referred to as Electron Spectroscopy for Chemical Analysis (ECSA). In contrast to UPS, it is often used for composition analysis, to determine what elemental composition is present at the surface of the material (quantity and types of elements).
XPS can measure elemental composition as well as the chemical and electronic state of the atoms within a material. XPS spectra are obtained by irradiating a solid surface with a beam of X-rays and measuring the kinetic energy of electrons that are emitted from the top 1-10 nm of the material.
XPS spectral lines are identified by the shell from which the electron was ejected (1s, 2s, 2p, etc.). The ejected photoelectron has kinetic energy: KE=hv-BE-! L electron falls to fill core level vacancy (step 1).
Surface Characterization: XPS is applied to study the surfaces of implants and medical devices, assessing factors such as coatings, corrosion, and biofouling.
Adventitious carbon contamination is commonly used as a charge reference for XPS spectra. C1s spectrum for contamination typically has C-C, C-O-C, and O-C=O. components. The C-C component may be set to a binding energy of 284.8eV, by default.
Typical Pass Energy Range: 5 eV to 300 eV. XPS instruments measure Kinetic Energies (KEs) of Photoelectrons and convert those KEs into Binding Energies (BEs) within the range: 0 eV to 1487 eV. ( for Al X-rays)

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