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the first step in XPS data processing for many samples is to fit the carbon 1s peak particularly if were going to use adventitious carbon as a charge correction this procedure that Im going to show here is a good starting point for fitting adventitious carbon and also a good starting point for fitting general organics on a surface the first step is to go into our quantification parameters box and were going to create a background on your regions and generally use a shirley background and well set our end points for the background and then under components were going to create a component and then three more and well just move those over the first peak will be our aliphatic component so thats carbon bound to carbon and carbon bound to hydrogen the second peak will be our alcohol and ether component so carbon down to single a bound to oxygen the third component will be ketones and the fourth will be esters and acid functionality the alcohol peak generally I set it at about 1.5 Ev