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energy calibration is performed using an option on the Spectrum processing dialogue window itamp;#39;s under the calibration property page and the idea of energy calibrating an XPS spectrum is that you perform a shift and the shift should be applied to all measurements that are made at the same time that is to say youamp;#39;ve got a set of oxygen Peaks here where you can see shifts are evident and each one of these rows represents a different measurement so if we look at the malum say you can see that thereamp;#39;s a similar sort of shift going on here and what about the carbon yes youamp;#39;ve got again a similar shift here so these shifts in the energy are consistent along these rows and the idea of the calibration is to work out what that shift needs to be to align all of these Peaks and one question might be that why do you get shifts in XPS Peaks and thereamp;#39;s a an explanation that a charge builds up on the sample because when you irradiate the sample with x-rays elec
