Blot id in XPS

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How to Blot id in XPS

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[Music] hi everyone my name is Josh today Im gonna show you how we do x-ray photoelectron spectroscopy or XPS it all happens right in this lab lets go ahead and take a look were in the XPS lab welcome this is our XPS apparatus its very large mostly what it does is make a vacuum thats what all the noise youre hearing is we use this operettas to learn about chemistry of samples by hitting them with a beam of light and then looking at the electrons that come off after weve excited them with that x-ray light Im gonna sit down right here and take a look at this machines vital statistics before I get started Ive got two pressure measurements over here and thats because theres actually two chambers in this machine theres one chamber where we do the analysis in one chamber where we insert the samples those two set pressures look pretty good theyre within spec Im gonna make a note of that and then Im going to think about how Im going to put my samples inside the vacuum Ive got

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What instruments are used in XPS?

An XPS instrument contains an x-ray source, sample stage, extraction lenses, analyzer, and detector housed in an ultra-high vacuum environment.

What is commonly used detector in XPS?

The most prevalent electron spectrometer for XPS is the hemispherical electron analyzer. They have high energy resolution and spatial selection of the emitted electrons.

How do you calculate binding energy in XPS?

calculate WF by simply subtract the binding energy of the secondary region from the total energy of the incident light：WF =hv ESE，however others subtract by the width of the binding energy from onset of the secondary electrons up to the Fermi edge.

What is XPS spectroscopy mainly based on?

X-ray photoelectron spectroscopy (XPS) is based on the photoelectric effect. Absorbed light can eject electrons (the photoelectrons) from the nanoparticle after a give energy threshold, which depends on the binding energy of the electrons.

How does XPS detector work?

XPS spectra are obtained by irradiating a solid surface with a beam of X-rays and measuring the kinetic energy of electrons that are emitted from the top 1-10 nm of the material. A photoelectron spectrum is recorded by counting ejected electrons over a range of kinetic energies.

How do you analyze XPS results?

How to interpret the data it generates Peaks from the XPS spectra give relative number of electrons with a specific binding energy. The shorter the peak, the less electrons represented. The greater the binding energy, the greater the attraction of that electron to the nucleus.

What is the detection limit of XPS?

In general, detection limits for XPS range from 0.1 to 1 atomic percent. However there are cases where limits could be much better or much worse. An article from Alexander Shard [1] gives an excellent look at detection limits in over 6000 binary systems for both Al and Mg X-ray sources.

What information can we get from XPS?

XPS can measure elemental composition as well as the chemical and electronic state of the atoms within a material. XPS spectra are obtained by irradiating a solid surface with a beam of X-rays and measuring the kinetic energy of electrons that are emitted from the top 1-10 nm of the material.

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