Blot background in XPS

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How to blot background in XPS

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Charles Zona (CZ): Hello, and welcome to another McCrone Group webinar. My name is Charles Zona, and today we are happy to welcome Doug Meier. Doug is going to talk to us about X-ray photoelectron spectroscopy, otherwise known as XPS. Before we get started I would like to give you a bit of Dougamp;#39;s background. Doug is a senior research scientist with McCrone Associates. He specializes in surface sensitive spectroscopies, such as Auger electron, X-ray photoelectron, infrared reflection absorption, thermal desorption, and low-energy electron diffraction. Doug was awarded the U.S. Department of Commerceamp;#39;s Silver Medal for his work in the development of conductometric chemical microsensor array technology for the detection of chemical warfare agents. He also has over ten years of micro beam analysis experience prior to joining McCrone Associates. Doug will field questions from the audience immediately following todayamp;#39;s presentation, and this webinar is being recorded

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What is a Shirley background?

The classic Shirley background assumes two background regions with constant intensity on both sides of the peak. This feature has been accounted for in deriving the cross-section function Eq.

What is a Shirley made of?

The Shirley Temple is probably the most famous mocktail ever. This classic mix of ginger ale and grenadine with a squeeze of lemon or lime topped with maraschino cherries is believed to be the worlds first mocktail. And its still alive and well today.

What elements are detectable in XPS?

When laboratory X-ray sources are used, XPS easily detects all elements except hydrogen and helium. The detection limit is in the parts per thousand range, but parts per million (ppm) are achievable with long collection times and concentration at top surface.

What is the Shirley approximation?

The Shirley approximation is calculated from the current Gaussian/Lorentzian shape and a polynomial b0+b1(x-E) is used to scale the background in order to provide a fit to the observed spectra.

What is a Shirley?

A Shirley Temple is a non-alcoholic mixed drink traditionally made with ginger ale and a splash of grenadine, and garnished with a maraschino cherry. Modern Shirley Temple recipes may substitute lemon-lime soda or lemonade and sometimes orange juice, in part or in whole.

What causes satellite peaks in XPS?

These satellite peaks arise from localized charge transfer excitations that accompany the creation of a core hole 2. The presence and intensity of these satellite peaks can be used to determine the covalent character of the interaction between the Cd cation and the oxygen ligands 3.

What background is the name Shirley?

The name Shirley comes from the Old English words scire, meaning shire, or scīr, bright, as well as lēah, meaning meadow or clearing. This gender-neutral title was initially for boys; however, Charlotte Bronts novel Shirley has popularized it as a chic name for girls since its publication in 1849.

What is depth profiling in XPS?

XPS depth profiling is the alternating between ion gun etching cycles and XPS analysis cycles. The technique provides semi-quantitative information on the elemental composition (at. %) as a function of depth. The binding and electronic states of atoms can also be analyzed as a function of depth.

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