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After adjusting the height and position of the sample using the optical camera, we use the X-ray gun and detector to find the optimum height for testing. Opening the manual control window, we select spectrum mode, hybrid lens, electrostatic lens for magnetic samples, highest pass energy for resolution, and slot aperture for maximum counts and electrons. In the acquisition tab, choose XPS type, snapshot binding energy, and a reference of interest. In the energy regions table, input elements with the highest counts.
