Adapt guide in XPS

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Aug 6th, 2022
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How to adapt guide in XPS

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hello everyone welcome to todayamp;#39;s webinar from physical electronics todayamp;#39;s topic is x-ray photoelectron spectroscopy xps 101 and the agenda will be first of all weamp;#39;ll talk a little bit about physical electronics or phi as we are known and then weamp;#39;ll get right into xps weamp;#39;ll look a little bit about the history of the technique the basics of xps a little on xps instrumentation and then the types of data that xps can provide we have multiple ion beam technologies for different types of applications and then weamp;#39;ll look at several applications as well and then finish up with some hard xps analysis weamp;#39;ll look at so a little bit about physical electronics so physical electronics is a world leader in surface analytical analytical equipment and we specialize primarily in primarily in xps or x-ray photoelectron spectroscopy and that also includes hard xps or hackspace we also have oj electron spectroscopy or ees and also time of flight sec

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X-ray photoelectron spectroscopy (XPS), also known as electron spectroscopy for chemical analysis (ESCA), is a technique for analyzing a materials surface chemistry. XPS can measure elemental composition as well as the chemical and electronic state of the atoms within a material.
XPS can detect submonolayer coverages, so proper sample handling is essential. As mentioned above, gloves should be worn and clean metal tweezers used to handle the sample without contacting the area of interest.
XPS Sample Preparation: Press the powder into clean, high purity indium foil. Dissolve the powder in a suitable solvent and then drop cast onto the surface of a clean silicon wafer. Sprinkle the powder onto the surface of sticky carbon conductive tape or pressed into a tablet for analysis.
The average depth of analysis for an XPS measurement is approximately 5 nm.
X-ray Photoelectron Spectroscopy (XPS) or Electron Spectroscopy for Chemical Analysis (ESCA) is a technique which analyzes the elements constituting the sample surface, its composition, and chemical bonding state by irradiating x-rays on the sample surface, and measuring the kinetic energy of the photoelectrons emitted
Because XPS is a surface technique, there is a limited amount of organic information XPS can provide. XPS is limited to measurements of elements having atomic numbers of 3 or greater, making it unable to detect hydrogen or helium. XPS spectra also take a long time to obtain.
How to interpret the data it generates Peaks from the XPS spectra give relative number of electrons with a specific binding energy. The shorter the peak, the less electrons represented. The greater the binding energy, the greater the attraction of that electron to the nucleus.

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