Change fact in XPS

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Upload your file to our editor. Select how you prefer - dragging and dropping it into our uploading pane, browsing from your device, the cloud, or via a secure link to a third-party resource.
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How to Change fact in XPS

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Charles Zona (CZ): Hello, and welcome to another McCrone Group webinar. My name is Charles Zona, and today we are happy to welcome Doug Meier. Doug is going to talk to us about X-ray photoelectron spectroscopy, otherwise known as XPS. Before we get started I would like to give you a bit of Dougs background. Doug is a senior research scientist with McCrone Associates. He specializes in surface sensitive spectroscopies, such as Auger electron, X-ray photoelectron, infrared reflection absorption, thermal desorption, and low-energy electron diffraction. Doug was awarded the U.S. Department of Commerces Silver Medal for his work in the development of conductometric chemical microsensor array technology for the detection of chemical warfare agents. He also has over ten years of micro beam analysis experience prior to joining McCrone Associates. Doug will field questions from the audience immediately following todays presentation, and this webinar is being recorded and will be available on

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What does higher binding energy mean XPS?

The greater the binding energy, the greater the attraction of that electron to the nucleus. i.e. peaks from electrons in 1s will have a greater energy than peaks representing electrons from 2s. Electrons in 2s will have greater energy than those in 2p.

What increases XPS spectroscopy binding energy?

Atoms of a higher positive oxidation state exhibit a higher binding energy due to the extra coulombic interaction between the photo-emitted electron and the ion core. This ability to discriminate between different oxidation states and chemical environments is one of the major strengths of the XPS technique.

What is the binding energy of carbon XPS?

The C-C component may be set to a binding energy of 284.8eV, by default.

What is the binding energy of iron in XPS?

The broad structure to higher binding energy (~710.5eV) of the main Fe2p3/2 peak is NOT satellite structure but is due to Fe3+ states from oxidation of the surface.

What does binding energy mean XPS?

The XPS binding energy of an atom is a measure of the electronic environment of the atom. Decreasing the electron density of an atom (such as a C-O bond compared with a C-C bond) increases the binding energy of the atom.

What is shake up and shake off in XPS?

Shake-up satellites: distinct peaks a few eV below the main line. Shake-off satellites: broad feature at lower energy w.r.t. to main line. energy loss). n: e density, e: charge of e, m: mass of e electron.

What does shift in XPS mean?

The shifts in the XPS peak is related to its oxidation state and higher shift in binding energy corresponds to higher oxidation state. Some times more shift with noise peak is related to the satellite peak or shake up and it is a case for only some metal or its oxide for example Ni or NiO.

How do you convert kinetic energy to binding energy in XPS?

The photoelectron kinetic energy (KE) excited by a photon energy (PE) is measured from a reference from the spectrometer workfunction (WF), so the binding energy (BE) is formulated as the following equation; PE = BE + (KE + WF).

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